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An easy and short preparation of pentachloroacetone by selective dechlorination of hexachloroacetone under Appel conditions
Rajendran, Kamalraj V.; Carr, Damien J.; Gilheany, Declan G.
We report a very convenient laboratory preparation of pentachloroacetone (PCA) by selective dechlorination of hexachloroacetone (HCA) via reaction with triphenylphosphine in the presence of methanol or aromatic alcohols. kpw14/11/13
Keyword(s): Hexachloroacetone; Pentachloroacetone; Triphenylphosphine; Appel reaction; Chlorophosphonium salt; Aryloxyphosphonium salt
Publication Date:
2013
Type: Journal article
Peer-Reviewed: Unknown
Language(s): English
Institution: University College Dublin
Publisher(s): Elsevier
First Indexed: 2013-11-16 05:17:20 Last Updated: 2018-10-11 16:51:19